Mass transfer and chemical test reactions in the continuous flow rotor-stator mixer

Magdalena Jasińska , Jerzy Robert Bałdyga , Michael Cooke , Adam J. Kowalski

Abstract

This work is on mass transfer in liquid-liquid two-phase systems. To study mass transfer in the continuous flow in-line rotor-stator mixer, a method based on experimental determination of the product distribution of a set of complex chemical reactions has been applied together with drop breakage experiments. Experiments were carried out using the high-shear rotor-stator Silverson mixer for both drop dispersion and intensification of mass transfer. Volume fraction of organic phase was in the range between 0.01 and 0.015. The product distribution of complex reactions was determined based on high-performance liquid chromatography measurements. The drop size distribution was measured with the Malvern MasterSizer just after the process. Results of modeling of mass transfer with chemical reaction were used to characterise energetic efficiency of mass transfer.
Author Magdalena Jasińska ZIDRCh
Magdalena Jasińska,,
- Department of Chemical Reactor Engineering and Dynamics
, Jerzy Robert Bałdyga ZIDRCh
Jerzy Robert Bałdyga,,
- Department of Chemical Reactor Engineering and Dynamics
, Michael Cooke
Michael Cooke,,
-
, Adam J. Kowalski
Adam J. Kowalski,,
-
Journal seriesTheoretical Foundations of Chemical Engineering, ISSN 0040-5795
Issue year2016
Vol50
No6
Pages901-906
Publication size in sheets0.5
Conference15th European Conference on Mixing, 28-06-2015 - 03-07-2015, Saint-Petersburg, Rosja
Keywords in Englishemulsion, energetic efficiency, mass transfer, rotor-stator mixer, test reactions
DOIDOI:10.1134/S0040579516060075
URL http://download.springer.com/static/pdf/347/art%253A10.1134%252FS0040579516060075.pdf?originUrl=http%3A%2F%2Flink.springer.com%2Farticle%2F10.1134%2FS0040579516060075&token2=exp=1481194353~acl=%2Fstatic%2Fpdf%2F347%2Fart%25253A10.1134%25252FS0040579516060075.pdf%3ForiginUrl%3Dhttp%253A%252F%252Flink.springer.com%252Farticle%252F10.1134%252FS0040579516060075*~hmac=dc8a1fbbd5952d9f261c53911ad75806ec18217a3e8185c4573f867328053738
Languageen angielski
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Jasińska M. (i in.) - Mass Transfer and Chemical...pdf 715.78 KB
Score (nominal)15
ScoreMinisterial score [Punktacja MNiSW] = 15.0, 28-11-2017, ArticleFromJournalAndMatConfByIndicator
Ministerial score (2013-2016) [Punktacja MNiSW (2013-2016)] = 15.0, 28-11-2017, ArticleFromJournalAndMatConfByIndicator
Publication indicators WoS Impact Factor [Impact Factor WoS]: 2016 = 0.494 (2) - 2016=0.554 (5)
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