Towards cubic modification of Li
7 La 3 Zr 2 O 12 compound by mechanical milling and annealing of powders
Dariusz Oleszak , B. Kurowski , T. Pikula , M. Pawlyta , M. Senna , H. Suzuki
The aim of these studies was to obtain single phase cubic modification of Li 7 La 3 Zr 2 O 12 by mechanical milling and annealing of La(OH) 3 , Li 2 CO 3 and ZrO 2 powder mixture. Fritsch P5 planetary ball mill, Rigaku MiniFlex II X-ray diffractometer, Setaram TG-DSC 1500 analyser and FEI Titan 80-300 transmission electron microscope were used for sample preparation and investigations. The applied milling and annealing parameters allowed to obtain the significant contribution of c-Li 7 La 3 Zr 2 O 12 in the sample structure, reaching 90%. Thermal measurements revealed more complex reactions requiring further studies.
|Journal series||Archives of Metallurgy and Materials, ISSN 1733-3490|
|Score||= 40.0, 26-05-2020, ArticleFromJournal|
|Publication indicators||= 0; : 2018 = 0.534; : 2018 = 0.697 (2) - 2018=0.72 (5)|
* presented citation count is obtained through Internet information analysis and it is close to the number calculated by the Publish or Perish system.