Synthesis of tin disulfide single crystals for nano-layer exfoliation

Maciej Białogłowski , Cezariusz Jastrzębski , Sławomir Podsiadło , Daniel J. Jastrzebski , Roman Gajda , Wojciech Gębicki , Patrycja A. Wrzosek , Krzysztof Wozniak

Abstract

Efficient and inexpensive method of chemical transport based on Ag2S catalyst was used to produce relatively large crystals of SnS2, up to 5 mm in linear size. Good quality of the obtained layered crystals of SnS2 was confirmed by X-ray, SEM, EDX and Raman measurements, however the layers appeared to be slightly twisted in relation to each other. Nanometric (down to c.a. 10 nm) layers of SnS2 on a Si substrate were obtained by mechanical exfoliation. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
Author Maciej Białogłowski (FC / CICSST)
Maciej Białogłowski,,
- Chair Of Inorganic Chemistry And Solid State Technology
, Cezariusz Jastrzębski (FP / SRD)
Cezariusz Jastrzębski,,
- Structural Research Division
, Sławomir Podsiadło (FC / CICSST)
Sławomir Podsiadło,,
- Chair Of Inorganic Chemistry And Solid State Technology
, Daniel J. Jastrzebski (FC / CICSST)
Daniel J. Jastrzebski,,
- Chair Of Inorganic Chemistry And Solid State Technology
, Roman Gajda
Roman Gajda,,
-
, Wojciech Gębicki (FP / SRD)
Wojciech Gębicki,,
- Structural Research Division
, Patrycja A. Wrzosek (FC / CICSST)
Patrycja A. Wrzosek,,
- Chair Of Inorganic Chemistry And Solid State Technology
, Krzysztof Wozniak
Krzysztof Wozniak,,
-
Journal seriesCrystal Research and Technology, ISSN 1521-4079 [0232-1300], (A 20 pkt)
Issue year2015
Vol50
No9-10 special issue
Pages695-699
Publication size in sheets0.5
Keywords in EnglishSemiconductor materials; Silver; Tin, Chemical transport; Exfoliation; Large crystal; Layered crystals; Mechanical exfoliation; Raman measurements; Si substrates; Tin disulfides, Single crystals
ASJC Classification3104 Condensed Matter Physics; 2500 General Materials Science; 1600 General Chemistry
DOIDOI:10.1002/crat.201400436
URL http://onlinelibrary.wiley.com/doi/10.1002/crat.201400436/abstract
LanguageEnglish
File
Bialoglowski_et_al-2015-Crystal_Research_and_Technology.pdf 487.27 KB
Score (nominal)20
ScoreMinisterial score = 20.0, 19-11-2018, ArticleFromJournal
Ministerial score (2013-2016) = 20.0, 19-11-2018, ArticleFromJournal
Publication indicators Scopus SNIP (Source Normalised Impact per Paper): 2017 = 0.573; WoS Impact Factor: 2017 = 1.122 (2) - 2017=1.059 (5)
Citation count*3 (2018-11-14)
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* presented citation count is obtained through Internet information analysis and it is close to the number calculated by the Publish or Perish system.
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