Data on synthesis and characterization of new diglycerol based environmentally friendly non-isocyanate poly(hydroxyurethanes)
Mariusz Tryznowski , Aleksandra Świderska , Zuzanna Żołek-Tryznowska , Tomasz Gołofit , Paweł Parzuchowski
AbstractThis article contains original experimental data, figures and methods to the preparation of non-isocyanate poly(hydroxyurethanes) by an environmentally friendly method without the use of toxic phosgene and isocyanates from bis(2,3-dihydroxypropyl)ether dicarbonate and various diamines (Tryznowski et al., Submitted for publication) . Bis(2,3-dihydroxypropyl)ether dicarbonate was obtained from a one-step procedure from commercially available diglycerol. The product was characterized by 1H NMR, 13C NMR, and FTIR spectroscopies and for the first time by X-Ray diffraction measurements. Then, the bis(cyclic carbonate) monomer was used as a precursor for the synthesis of various NIPUs. The NIPUs were prepared in a non-solvent process. Spectral and thermal properties of the NIPUs are compered. Here we give the procedure in order to perform bis(2,3-dihydroxypropyl)ether dicarbonate with high yield and the procedure NIPU synthesis and the complete set of monomer and NIPU analysis (1H NMR, 13C NMR, FTIR, X-Ray). © 2015.
|Journal series||Data in Brief, ISSN 2352-3409|
|Publication size in sheets||0.5|
|Score|| = 0.0, 28-11-2017, ArticleFromJournal|
= 0.0, 28-11-2017, ArticleFromJournal - czasopismo zagraniczne spoza list
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