Data on synthesis and characterization of new diglycerol based environmentally friendly non-isocyanate poly(hydroxyurethanes)

Mariusz Tryznowski , Aleksandra Świderska , Zuzanna Żołek-Tryznowska , Tomasz Gołofit , Paweł Parzuchowski

Abstract

This article contains original experimental data, figures and methods to the preparation of non-isocyanate poly(hydroxyurethanes) by an environmentally friendly method without the use of toxic phosgene and isocyanates from bis(2,3-dihydroxypropyl)ether dicarbonate and various diamines (Tryznowski et al., Submitted for publication) [1]. Bis(2,3-dihydroxypropyl)ether dicarbonate was obtained from a one-step procedure from commercially available diglycerol. The product was characterized by 1H NMR, 13C NMR, and FTIR spectroscopies and for the first time by X-Ray diffraction measurements. Then, the bis(cyclic carbonate) monomer was used as a precursor for the synthesis of various NIPUs. The NIPUs were prepared in a non-solvent process. Spectral and thermal properties of the NIPUs are compered. Here we give the procedure in order to perform bis(2,3-dihydroxypropyl)ether dicarbonate with high yield and the procedure NIPU synthesis and the complete set of monomer and NIPU analysis (1H NMR, 13C NMR, FTIR, X-Ray). © 2015.
Author Mariusz Tryznowski KChTP
Mariusz Tryznowski,,
- Chair Of Polymer Chemistry And Technology
, Aleksandra Świderska KChTP
Aleksandra Świderska,,
- Chair Of Polymer Chemistry And Technology
, Zuzanna Żołek-Tryznowska IMP
Zuzanna Żołek-Tryznowska,,
- The Institute of Mechanics and Printing
, Tomasz Gołofit ZMW
Tomasz Gołofit,,
- Department Of High-Energetic Materials
, Paweł Parzuchowski KChTP
Paweł Parzuchowski,,
- Chair Of Polymer Chemistry And Technology
Journal seriesData in Brief, ISSN 2352-3409
Issue year2016
Vol6
Pages77-82
Publication size in sheets0.5
DOIDOI:10.1016/j.dib.2015.11.034
URL http://www.sciencedirect.com/science/article/pii/S2352340915003297
LanguageEnglish
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Ministerial score (2013-2016) = 0.0, 28-11-2017, ArticleFromJournal - czasopismo zagraniczne spoza list
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