Data on synthesis and characterization of new diglycerol based environmentally friendly non-isocyanate poly(hydroxyurethanes)

Mariusz Tryznowski , Aleksandra Świderska , Zuzanna Żołek-Tryznowska , Tomasz Gołofit , Paweł Parzuchowski


This article contains original experimental data, figures and methods to the preparation of non-isocyanate poly(hydroxyurethanes) by an environmentally friendly method without the use of toxic phosgene and isocyanates from bis(2,3-dihydroxypropyl)ether dicarbonate and various diamines (Tryznowski et al., Submitted for publication) [1]. Bis(2,3-dihydroxypropyl)ether dicarbonate was obtained from a one-step procedure from commercially available diglycerol. The product was characterized by 1H NMR, 13C NMR, and FTIR spectroscopies and for the first time by X-Ray diffraction measurements. Then, the bis(cyclic carbonate) monomer was used as a precursor for the synthesis of various NIPUs. The NIPUs were prepared in a non-solvent process. Spectral and thermal properties of the NIPUs are compered. Here we give the procedure in order to perform bis(2,3-dihydroxypropyl)ether dicarbonate with high yield and the procedure NIPU synthesis and the complete set of monomer and NIPU analysis (1H NMR, 13C NMR, FTIR, X-Ray). © 2015.
Author Mariusz Tryznowski (FC / CPCT)
Mariusz Tryznowski,,
- Chair Of Polymer Chemistry And Technology
, Aleksandra Świderska (FC / CPCT)
Aleksandra Świderska,,
- Chair Of Polymer Chemistry And Technology
, Zuzanna Żołek-Tryznowska (FPE / IMP)
Zuzanna Żołek-Tryznowska,,
- The Institute of Mechanics and Printing
, Tomasz Gołofit (FC / DH-EM)
Tomasz Gołofit,,
- Department Of High-Energetic Materials
, Paweł Parzuchowski (FC / CPCT)
Paweł Parzuchowski,,
- Chair Of Polymer Chemistry And Technology
Journal seriesData in Brief, ISSN 2352-3409
Issue year2016
Publication size in sheets0.5
main.pdf 631.09 KB
Score (nominal)0
ScoreMinisterial score = 0.0, 05-09-2019, ArticleFromJournal
Ministerial score (2013-2016) = 0.0, 05-09-2019, ArticleFromJournal
Publication indicators WoS Citations = 1; Scopus Citations = 1
Citation count*2 (2020-08-24)
Share Share

Get link to the record

* presented citation count is obtained through Internet information analysis and it is close to the number calculated by the Publish or Perish system.
Are you sure?