Thermal expansion of CuInSe2 in the 11-1,073 K range: an X-ray diffraction study

W Paszkowicz , R. Minikayev , P. Piszora , D. Trots , M. Knapp , Tomasz Wojciechowski , Rajmund Bacewicz

Abstract

Structural and elastic properties of chalcopyrite-type CuInSe2 are determined in almost full stability range of temperature from 11 to 1,073 K, by in situ X-ray diffraction, employing a synchrotron-radiation source. The studied polycrystalline sample was prepared from a stoichiometric single crystal. Phase analysis reveals the formation of a trace amount of indium oxide impurity phase at the highest temperatures studied. From the obtained smooth lattice-parameter dependencies on temperature, the temperature dependencies of thermal expansion coefficients are derived. These coefficients are found to follow the trends previously reported for narrow temperature intervals. The present results provide a clear experimental evidence that the linear expansion coefficient is slightly negative below 47 K in both, a and c, directions; this temperature limit is in between the previously reported theoretical value (35 K) and the experimental ones (60 and 80 K) of such limit. © 2013 The Author(s).
Author W Paszkowicz - [Institute of Physics of the Polish Academy of Sciences]
W Paszkowicz,,
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, R. Minikayev - [Institute of Physics of the Polish Academy of Sciences]
R. Minikayev,,
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, P. Piszora - [Adam Mickiewicz University (UAM)]
P. Piszora,,
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- Uniwersytet im. Adama Mickiewicza w Poznaniu
, D. Trots - [University of Bayreuth, Bayerisches Geoinstitut]
D. Trots,,
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, M. Knapp - [Karlsruhe Institute of Technology]
M. Knapp,,
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, Tomasz Wojciechowski - [Institute of Physics of the Polish Academy of Sciences]
Tomasz Wojciechowski,,
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, Rajmund Bacewicz (FP / SD)
Rajmund Bacewicz,,
- Semiconductors Division
Journal seriesApplied Physics A-Materials Science & Processing, ISSN 0947-8396
Issue year2013
Vol116
Pages767-780
Publication size in sheets0.65
ASJC Classification2500 General Materials Science; 1600 General Chemistry
DOIDOI:10.1007/s00339-013-8146-9
URL http://www.scopus.com/inward/record.url?eid=2-s2.0-84890930637&partnerID=40&md5=8fee5f9b9dd9efa7e81ce05e6e38f701
LanguageEnglish
Score (nominal)30
Score sourcejournalList
ScoreMinisterial score = 30.0, 10-06-2020, ArticleFromJournal
Ministerial score (2013-2016) = 30.0, 10-06-2020, ArticleFromJournal
Publication indicators WoS Citations = 5; Scopus Citations = 6; Scopus SNIP (Source Normalised Impact per Paper): 2013 = 0.993; WoS Impact Factor: 2013 = 1.694 (2) - 2013=1.713 (5)
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