Enhancement of supercritical fluid extraction in membrane cleaning process by addition of organic solvents

Jan Krzysztoforski , Andrzej Ryszard Krasiński , Marek Henczka , Wojciech Piątkiewicz

Abstract

In this study, the process of membrane cleaning by supercritical fluid extraction was investigated. Polypropylene microfiltration membranes, contaminated with oils, were treated in a batch process with a supercritical fluid (SCF). As extractant, pure supercritical carbon dioxide or supercritical carbon dioxide with admixtures of methanol, ethanol and isopropanol were used. Single-stage and multi-stage extraction was carried out and process efficiency was determined. The obtained results showed that addition of organic solvents significantly enhances the cleaning performance, which increases with increase of organic solvent concentration and decreases with increasing temperature. All three solvents showed a comparable effect of efficiency enhancement. The results confirmed that supercritical fluid extraction can be applied for polypropylene membrane cleaning.
Author Jan Krzysztoforski (FCPE / DCRED)
Jan Krzysztoforski,,
- Department of Chemical Reactor Engineering and Dynamics
, Andrzej Ryszard Krasiński (FCPE / CIPE)
Andrzej Ryszard Krasiński,,
- Chair of Integrated Process Engineering
, Marek Henczka (FCPE / DCRED)
Marek Henczka,,
- Department of Chemical Reactor Engineering and Dynamics
, Wojciech Piątkiewicz (FCPE / CIPE)
Wojciech Piątkiewicz,,
- Chair of Integrated Process Engineering
Journal seriesChemical and Process Engineering , [Inżynieria Chemiczna i Procesowa], ISSN 0208-6425
Issue year2013
Vol34
No3
Pages403-414
Publication size in sheets0.55
Keywords in Polishpłyn nadkrytyczny, wydobycie, membrana porowata
Keywords in Englishsupercritical fluid, extraction, porous membrane, TIPS
ASJC Classification1500 General Chemical Engineering; 1600 General Chemistry
DOIDOI:10.2478/cpe-2013-0033
URL http://www.degruyter.com/view/j/cpe.2013.34.issue-3/cpe-2013-0033/cpe-2013-0033.xml
Languageen angielski
File
Krzysztoforski J. (i in.) - Enhancement of supercritical....pdf 491.29 KB
Score (nominal)15
Score sourcejournalList
ScoreMinisterial score = 15.0, 11-05-2020, ArticleFromJournal
Ministerial score (2013-2016) = 15.0, 11-05-2020, ArticleFromJournal
Publication indicators WoS Citations = 5; Scopus Citations = 4; GS Citations = 7.0; Scopus SNIP (Source Normalised Impact per Paper): 2013 = 0.622; WoS Impact Factor: 2013 = 0.467 (2) - 2013=0.408 (5)
Citation count*7 (2020-09-07)
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* presented citation count is obtained through Internet information analysis and it is close to the number calculated by the Publish or Perish system.
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