Application of test reactions to study micromixing in the rotor-stator mixer (test reactions for rotor-stator mixer)

Magdalena Jasińska , Jerzy Robert Bałdyga , Michael Cooke , Adam Kowalski

Abstract

Rotor-stator devices are known from their ability to generate very high shear stresses; due to focused delivery of energy, their energetic efficiency is regarded as high. In the present work performance of the Silverson double screen 150/250MS inline rotor-stator mixer is investigated using multiple test reactions (a simultaneous diazo coupling between 1- and 2-naphtols and diazotized sulphanilic acid), power measurements and CFD. In experiments a premixture of 1- and 2-naphtols was fed into the system through the main inlet whereas second reagent was introduced through the separate feeding tube. Experiments were carried out for the total volumetric flow rate equal to 0.1 dm3 s−1, the volume ratio of reactant solutions equal to 15, and for the rotor speed from the range between 500 and 9000 rpm. The hydrodynamics, mixing and the course of chemical reactions in the rotor-stator mixer are simulated using the standard k–ε model of Ansys Fluent and the multi-reference frame approach. The presented model is able to properly predict the power input to the rotor-stator system and details of turbulence structure, which was confirmed by comparing experimental data with model predictions for power input and product distributions.
Author Magdalena Jasińska (FCPE / DCRED)
Magdalena Jasińska,,
- Department of Chemical Reactor Engineering and Dynamics
, Jerzy Robert Bałdyga (FCPE / DCRED)
Jerzy Robert Bałdyga,,
- Department of Chemical Reactor Engineering and Dynamics
, Michael Cooke - [University of Manchester]
Michael Cooke,,
-
-
, Adam Kowalski - [Unilever]
Adam Kowalski,,
-
-
Journal seriesApplied Thermal Engineering, ISSN 1359-4311
Issue year2013
Vol57
No1-2
Pages172-179
Publication size in sheets0.5
Keywords in Englishin-line high-shear mixer, micromixing, power number, rotor-stator mixer, test reactions
ASJC Classification2209 Industrial and Manufacturing Engineering; 2102 Energy Engineering and Power Technology
DOIDOI:10.1016/j.applthermaleng.2012.06.036
URL http://www.sciencedirect.com/science/article/pii/S1359431112004577
Languageen angielski
File
Jasińska M. (i in.) - Application of test....pdf 2.08 MB
Score (nominal)40
Score sourcejournalList
ScoreMinisterial score = 35.0, 29-04-2020, ArticleFromJournal
Ministerial score (2013-2016) = 40.0, 29-04-2020, ArticleFromJournal
Publication indicators WoS Citations = 22; Scopus Citations = 24; GS Citations = 3.0; Scopus SNIP (Source Normalised Impact per Paper): 2013 = 2.457; WoS Impact Factor: 2013 = 2.624 (2) - 2013=2.88 (5)
Citation count*3 (2015-04-23)
Cite
Share Share

Get link to the record


* presented citation count is obtained through Internet information analysis and it is close to the number calculated by the Publish or Perish system.
Back
Confirmation
Are you sure?